5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

Base Information

Chemical Name:5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin
CAS No.:85304-61-6
Molecular Formula:C₆₅H₅₀N₁₀O₄
Molecular Weight:1035.18
Hs Code.:

Synonyms:5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

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Chemical Property of 5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

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Technology Process of 5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

There total 6 articles about 5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52199-35-6
tetrakis-5,10,15,20-(o-aminophenyl)porphyrin

: 85304-61-6
5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / triethylamine / CH₂Cl₂ / 2 h

2: 33 percent / pyridine / CH₂Cl₂

3: 90percent acetic acid

4: 2.) pyridine / 1.) THF, 20 min, 2.) 2 h

With pyridine; acetic acid; triethylamine; In dichloromethane;
DOI:10.1021/ja00348a018

Reference yield:

: 4435-67-0
1,3,5-benzenetriacetic acid

: 85304-61-6
5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂, DMF / 24 h / Ambient temperature

2: 33 percent / pyridine / CH₂Cl₂

3: 90percent acetic acid

4: 2.) pyridine / 1.) THF, 20 min, 2.) 2 h

With pyridine; thionyl chloride; acetic acid; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ja00348a018

Reference yield:

: 77354-22-4
1,3,5-benzene-triacetyl chloride

: 85304-61-6
5,10,15-((1,3,5-benzenetriyltriacetyl)tris(α,α,α-o-aminophenyl))-20-(β-o-3-(N-pyridyl)propylureidophenyl)porphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / pyridine / CH₂Cl₂

2: 90percent acetic acid

3: 2.) pyridine / 1.) THF, 20 min, 2.) 2 h

With pyridine; acetic acid; In dichloromethane;
DOI:10.1021/ja00348a018