N-(1-naphthyl)-N',N'-diethylethylenediamine

Base Information

• Chemical Name: N-(1-naphthyl)-N',N'-diethylethylenediamine
• CAS No.: 5235-86-9
• Molecular Formula: C16H22 N2
• Molecular Weight: 242.36
• Mol file: 5235-86-9.mol

Synonyms:1,2-Ethanediamine,N,N-diethyl-N'-1-naphthalenyl- (9CI); Ethylenediamine,N,N-diethyl-N'-1-naphthyl- (7CI,8CI);N,N-Diethyl-N'-(1-naphthyl)-1,2-ethanediamine;N,N-Diethyl-N'-(1-naphthyl)ethylenediamine; N,N-Diethyl-N'-(a-naphthyl)ethylenediamine;N-(1-Naphthyl)-N'-diethylethylenediamine;N-(2-Diethylaminoethyl)-1-naphthylamine

Chemical Property of N-(1-naphthyl)-N',N'-diethylethylenediamine

Chemical Property:

• Boiling Point: 386.8°Cat760mmHg
• Flash Point: 155.6°C
• PSA: 15.27000
• Density: 1.041g/cm³
• LogP: 3.66650

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(1-naphthyl)-N',N'-diethylethylenediamine

There total 5 articles about N-(1-naphthyl)-N',N'-diethylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-N,N-diethylethylamine hydrochloride (869-24-9) + 1-amino-naphthalene (134-32-7) → N,N-diethyl-N'-(1-naphthalenyl)-1,2-ethanediamine (5235-86-9)

Guidance literature:

With copper; potassium carbonate; benzene;

DOI:10.1021/ja01216a017

Reference yield:

2-(Diethylamino)ethanol (100-37-8) → N,N-diethyl-N'-(1-naphthalenyl)-1,2-ethanediamine (5235-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃

2: K₂CO₃ / toluene

With thionyl chloride; potassium carbonate; In chloroform; toluene;

DOI:10.1016/j.bmcl.2003.12.086

Reference yield:

1-amino-naphthalene (134-32-7) + 2-(diethylamino)ethyl chloride (100-35-6) → N,N-diethyl-N'-(1-naphthalenyl)-1,2-ethanediamine (5235-86-9)

Guidance literature:

With benzene;

upstream raw materials:

2-chloro-N,N-diethylethylamine hydrochloride

1-amino-naphthalene

2-(diethylamino)ethyl chloride

2-(Diethylamino)ethanol

Downstream raw materials:

N-<2-(diethylamino)ethyl>-4-(1H-imidazol-1-yl)-4-(1-naphthalenyl)benzamide

N-<2-(diethylamino)ethyl>-4-fluoro-N-(1-naphthalenyl)benzamide

N-<2-(diethylamino)ethyl>-4-<(methylsulfonyl)amino>-N-(1-naphthalenyl)benzamide

Refernces