(E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

Base Information

Chemical Name:(E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide
CAS No.:1403954-96-0
Molecular Formula:C₁₄H₁₃NO
Molecular Weight:211.263
Hs Code.:

Synonyms:(E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

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Chemical Property of (E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

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Technology Process of (E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

There total 4 articles about (E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2403-02-3
4-carboxy-2-nitropyridine N-oxide

: 1730-25-2,13154-14-8,13154-15-9,14092-04-7
(E)-1-propenylmagnesium bromide

: 100-58-3
phenylmagnesium bromide

: 1403954-96-0
(E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

Guidance literature:: 4-carboxy-2-nitropyridine N-oxide; phenylmagnesium bromide; In tetrahydrofuran; at -50 ℃;

(E)-1-propenylmagnesium bromide; In tetrahydrofuran; at -50 ℃;

With phosphorus trichloride; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1021/ol3026632

Reference yield:

: 1008-89-5
2-phenylpyridine

: 1403954-96-0
(E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere

2: palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate; potassium fluoride / tetrahydrofuran / 24 h / 100 °C / Inert atmosphere

With potassium fluoride; palladium diacetate; 3-chloro-benzenecarboperoxoic acid; tri tert-butylphosphoniumtetrafluoroborate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/acs.orglett.8b00689

Reference yield:

: 15009-91-3,1232169-16-2
2-nitropyridine

: 1403954-96-0
(E)-2-phenyl-6-(prop-1-enyl)pyridine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: carbamide peroxide; trifluoroacetic anhydride / dichloromethane / 0 - 20 °C

2.1: tetrahydrofuran / -50 °C

2.2: -50 °C

2.3: 2 h / 0 - 20 °C

With carbamide peroxide; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol3026632