4-[(2,4-diamino-5-methyl-phenyl)methyl]-6-methyl-benzene-1,3-diamine

Base Information

• Chemical Name: 4-[(2,4-diamino-5-methyl-phenyl)methyl]-6-methyl-benzene-1,3-diamine
• CAS No.: 97-22-3
• Molecular Formula: C15H20N4
• Molecular Weight: 256.351
• Hs Code.: 2921519090
• Mol file: 97-22-3.mol

Synonyms:Bis(3-methyl-4,6-diaminophenyl)methane;Methylenebis(toluenediamine);4.6.4'.6'-Tetraamino-3.3'-dimethyl-diphenylmethan;Bis(2,4-tolylenediamine)methane;Bis(2,4-TDA)methane;Tetraaminoditolylmethane;bis-(2,4-diamino-5-methyl-phenyl)-methane;

Chemical Property of 4-[(2,4-diamino-5-methyl-phenyl)methyl]-6-methyl-benzene-1,3-diamine

Chemical Property:

• Melting Point: 181-183oC
• Boiling Point: 524oC at 760 mmHg
• Flash Point: 307.5oC
• PSA: 104.08000
• Density: 1.217g/cm3
• LogP: 4.54780
• Storage Temp.: -20°C Freezer, Under Inert Atmosphere
• Solubility.: DMSO, Methanol

Purity/Quality:

Bis(2,4-diamino-5-methylphenyl)methane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: It is formed by interaction of methanol and the aromatic amine 2,4-diaminotoluene. A new mutagenic compound.

Technology Process of 4-[(2,4-diamino-5-methyl-phenyl)methyl]-6-methyl-benzene-1,3-diamine

There total 2 articles about 4-[(2,4-diamino-5-methyl-phenyl)methyl]-6-methyl-benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-methylbenzene-1,3-diamine (95-80-7,71111-07-4) → 6,6'-methylenebis[4-methyl-1,3-benzenediamine] (97-22-3)

Guidance literature:

With sulfuric acid;

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + sulfuric acid (7664-93-9) + 4-methylbenzene-1,3-diamine (95-80-7,71111-07-4) → 6,6'-methylenebis[4-methyl-1,3-benzenediamine] (97-22-3)

Guidance literature:

Reference yield:

6,6'-methylenebis[4-methyl-1,3-benzenediamine] (97-22-3) → acridine yellow (6441-73-2)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrochloric acid / 150 °C / nachfolgendes Oxydieren mit Eisenchlorid

2: nitrobenzene / Umsetzen mit Natriumchlorid

With hydrogenchloride; nitrobenzene;

upstream raw materials:

formaldehyd

4-methylbenzene-1,3-diamine

sulfuric acid

Downstream raw materials:

acridine yellow G

acridine yellow