N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside
CAS No.:1356933-25-9
Molecular Formula:C₁₈H₂₃NO₉
Molecular Weight:397.382
Hs Code.:

Synonyms:N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

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Chemical Property of N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

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Technology Process of N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

There total 16 articles about N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1376933-98-0
C₂₁H₂₇NO₉

: 1356933-25-9
N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

Guidance literature:: With acetic acid; In water; at 37 ℃; for 2h;
DOI:10.1021/jo202123s

Reference yield:

: 98911-14-9
N-phenylacetohydroxamic acid 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 1356933-26-0
N-phenylacetohydroxamic acid 2,4-di-O-acetyl-β-D-glucopyranoside

: 1356933-25-9
N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: Aspergillus niger lipase AS Amano; Streptomyces rochei carboxylesterase; water / dimethyl sulfoxide / 5 h / 40 °C / pH 7.2 / aq. phosphate buffer; Enzymatic reaction

2.1: pyridine; mono-4-methoxytrityl chloride / 16 h / 25 °C

2.2: 27 h / 25 °C

2.3: 3 h / 20 °C

3.1: Aspergillus niger lipase AS Amano; water / dimethyl sulfoxide / 40 °C / pH 5 / aq. acetate buffer; Enzymatic reaction

With pyridine; Aspergillus niger lipase AS Amano; Streptomyces rochei carboxylesterase; water; mono-4-methoxytrityl chloride; In dimethyl sulfoxide;
DOI:10.1021/jo202123s

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1356933-26-0
N-phenylacetohydroxamic acid 2,4-di-O-acetyl-β-D-glucopyranoside

: 1356933-25-9
N-phenylacetohydroxamic acid 2,3-di-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / ethanol; water / 1 h / 25 °C

2.1: Aspergillus niger lipase AS Amano; Streptomyces rochei carboxylesterase; water / dimethyl sulfoxide / 5 h / 40 °C / pH 7.2 / aq. phosphate buffer; Enzymatic reaction

3.1: pyridine; mono-4-methoxytrityl chloride / 16 h / 25 °C

3.2: 27 h / 25 °C

3.3: 3 h / 20 °C

4.1: Aspergillus niger lipase AS Amano; water / dimethyl sulfoxide / 40 °C / pH 5 / aq. acetate buffer; Enzymatic reaction

With pyridine; Aspergillus niger lipase AS Amano; Streptomyces rochei carboxylesterase; water; mono-4-methoxytrityl chloride; potassium hydroxide; In ethanol; water; dimethyl sulfoxide;
DOI:10.1021/jo202123s