(R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

Base Information

Chemical Name:(R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide
CAS No.:170801-80-6
Molecular Formula:C₁₈H₂₉NO₆
Molecular Weight:355.431
Hs Code.:

Synonyms:(R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

Suppliers and Price of (R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

Chemical Property:

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Technology Process of (R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

There total 4 articles about (R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 41365-75-7
aminopropane diethyl acetal

: 54814-41-4,54640-00-5,54910-31-5
3-(3,4-dimethoxy-phenyl)-2-hydroxy-propionic acid methyl ester

: 170801-80-6
(R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

Guidance literature:: With toluene-4-sulfonic acid; at 140 ℃; for 2h;
DOI:10.1002/ardp.19953280604

Reference yield:

: 2032-34-0
3,3-bis(ethyloxy)propanenitrile

: 170801-80-6
(R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / LiAlH₄ / diethyl ether / 16 h / Ambient temperature

2: 99 percent / p-TsOH / 2 h / 140 °C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether;
DOI:10.1002/ardp.19953280604

Reference yield:

: 153381-08-9
Methyl (S)-(+)-3-(3,4 dimethoxyphenyl)-2-hydroxypropionate

: 170801-80-6
(R)-(+)-N-(3,3-Diethoxypropyl)-3-(3,4-dimethoxyphenyl)-2-hydroxypropionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Ph₃P, DEAD / tetrahydrofuran; toluene / 18 h / Ambient temperature

2: 81 percent / NaOMe / methanol / 24 h / Ambient temperature

3: 99 percent / p-TsOH / 2 h / 140 °C

With sodium methylate; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; toluene;
DOI:10.1002/ardp.19953280604