(4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Base Information

Chemical Name:(4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene
CAS No.:445423-06-3
Molecular Formula:C₂₅H₄₄O₃Si
Molecular Weight:420.708
Hs Code.:

Synonyms:(4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Suppliers and Price of (4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

There total 7 articles about (4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 862475-43-2
(4R,6S,8R)-8-benzyloxy-2-ethyl-6-methoxy-non-1-en-4-ol

: 445423-06-3
(4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1039/b504148a

Reference yield:

: 445423-04-1
(2R,4R,6R)-2-benzyloxy-8-ethyl-6-propionoxy-8-nonen-4-ol

: 445423-06-3
(4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / proton-sponge / CH₂Cl₂ / 3 h / 0 °C

2: 88 percent / K₂CO₃ / methanol / 48 h / 20 °C

3: 95 percent / imidazole / dimethylformamide / 16 h / 20 °C

With 1H-imidazole; Proton-Sponge; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b504148a

Reference yield:

: 445423-05-2
(4R,6R,8R)-8-benzyloxy-2-ethyl-6-methoxy-4-propionoxy-1-nonene

: 445423-06-3
(4R,6R,8R)-8-benzyloxy-4-(t-butyldimethylsiloxy)-2-ethyl-6-methoxy-1-nonene

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₂CO₃ / methanol / 48 h / 20 °C

2: 95 percent / imidazole / dimethylformamide / 16 h / 20 °C

With 1H-imidazole; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1039/b504148a