1-phenyl-3-cyclopropylpropane

Base Information

• Chemical Name: 1-phenyl-3-cyclopropylpropane
• CAS No.: 58249-47-1
• Molecular Formula: C₁₂H₁₆
• Molecular Weight: 160.259
• Mol file: 58249-47-1.mol

Synonyms:1-phenyl-3-cyclopropylpropane

Chemical Property of 1-phenyl-3-cyclopropylpropane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1-phenyl-3-cyclopropylpropane

There total 7 articles about 1-phenyl-3-cyclopropylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

ethyl 3-phenylpropyl ketone (58977-36-9) → 1-phenyl-3-cyclopropylpropane (58249-47-1)

Guidance literature:

With nickel; In ethanol; Heating; acetone, reflux;

DOI:10.1016/S0040-4039(00)87347-5

Reference yield: 79.0%

cyclopropyl bromide (4333-56-6,130561-87-4) + 3-phenylpropyl 4-methylbenzenesulfonate (3742-75-4) → 1-phenyl-3-cyclopropylpropane (58249-47-1)

Guidance literature:

With copper(l) iodide; lithium methanolate; magnesium; bis-diphenylphosphinomethane; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere; Schlenk technique;

DOI:10.1002/chem.201405223

Reference yield:

(5-bromo-4-bromomethyl-pentyl)-benzene → 1-phenyl-3-cyclopropylpropane (58249-47-1) + isohexylbenzene (4215-86-5)

Guidance literature:

With titanocene(II) triethylphosphite complex; In tetrahydrofuran; at 0 ℃; for 3h; Title compound not separated from byproducts;

DOI:10.1246/cl.2002.290

upstream raw materials:

ethyl 3-phenylpropyl ketone

cyclopropyl bromide

Phenyl vinyl ketone

C₁₈H₂₀S