C₃₀H₄₇NO₇

Base Information

Chemical Name:C₃₀H₄₇NO₇
CAS No.:1309922-68-6
Molecular Formula:C₃₀H₄₇NO₇
Molecular Weight:533.706
Hs Code.:

C<sub>30</sub>H<sub>47</sub>NO<sub>7</sub>

Synonyms:C₃₀H₄₇NO₇

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Chemical Property of C₃₀H₄₇NO₇

Chemical Property:

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Technology Process of C₃₀H₄₇NO₇

There total 12 articles about C₃₀H₄₇NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1309922-67-5
C₂₅H₃₇N₃O₆

: 1309922-68-6
C₃₀H₄₇NO₇

Guidance literature:: With hydrogen; triethylamine; palladium 10% on activated carbon; In ethanol; water; for 16h; under 3102.97 Torr; Product distribution / selectivity;

Reference yield:

: 3969-84-4
3,4-di-O-isopropylidene-D-mannitol

: 1309922-68-6
C₃₀H₄₇NO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium periodate; sodium hydrogencarbonate / water / 3 h / 0 - 8 °C

1.2: 17 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

3.1: trifluoroacetic acid / acetonitrile; water / 6 h / Reflux

4.1: lithium hexamethyldisilazane; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran / 3 h / -78 °C

4.2: 3 h / -78 °C

5.1: pyridine; trichlorophosphate / 12.5 h / 10 - 20 °C

5.2: 0 °C / pH 5.5

6.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

7.1: n-butyllithium; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran; TETRAHYDROPYRANE / 1.33 h / -78 °C

7.2: 1.33 h / -78 °C

7.3: -78 °C / pH 7

8.1: triethylamine / dichloromethane / -10 °C

9.1: tetra(n-butyl)ammonium hydrogensulfate; sodium azide / N,N-dimethyl-formamide / 36 h / 90 °C

10.1: triethylamine; hydrogen / palladium 10% on activated carbon / ethanol; water / 16 h / 3102.97 Torr

With pyridine; sodium periodate; n-butyllithium; sodium azide; N²,N²-dimethyl-2-methyl-1,2-propanediamine; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; TETRAHYDROPYRANE; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 166239-53-8
(E)-3-[(4R,5R)-5-((E)-2-Ethoxycarbonyl-vinyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-acrylic acid ethyl ester

: 1309922-68-6
C₃₀H₄₇NO₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

2.1: trifluoroacetic acid / acetonitrile; water / 6 h / Reflux

3.1: lithium hexamethyldisilazane; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran / 3 h / -78 °C

3.2: 3 h / -78 °C

4.1: pyridine; trichlorophosphate / 12.5 h / 10 - 20 °C

4.2: 0 °C / pH 5.5

5.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

6.1: n-butyllithium; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran; TETRAHYDROPYRANE / 1.33 h / -78 °C

6.2: 1.33 h / -78 °C

6.3: -78 °C / pH 7

7.1: triethylamine / dichloromethane / -10 °C

8.1: tetra(n-butyl)ammonium hydrogensulfate; sodium azide / N,N-dimethyl-formamide / 36 h / 90 °C

9.1: triethylamine; hydrogen / palladium 10% on activated carbon / ethanol; water / 16 h / 3102.97 Torr

With pyridine; n-butyllithium; sodium azide; N²,N²-dimethyl-2-methyl-1,2-propanediamine; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; TETRAHYDROPYRANE; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;