8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

Base Information

Chemical Name:8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine
CAS No.:97423-26-2
Molecular Formula:C₂₄H₁₉ClN₄O
Molecular Weight:414.894
Hs Code.:

Synonyms:8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

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Chemical Property of 8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

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Technology Process of 8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

There total 4 articles about 8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 75-09-2
dichloromethane

: 18091-89-9,112393-62-1
7-chloro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine

: 97423-26-2
8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

Guidance literature:: In tetrahydrofuran; 1,1'-carbonyldiimidazole;

Reference yield:

: (4-Methoxy-phenyl)-acetic acid N'-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-hydrazide

: 97423-26-2
8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

Guidance literature:: With acetic acid; for 3h; Yield given; Heating;
DOI:10.1021/jm00126a003

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 97423-26-2
8-chloro-1-(4-methoxyphenylmethyl)-6-phenyl-4H-[1,2,4]triazolo[4,3-a][1,4]benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,1'-carbonyldiimidazole / 1.) THF, 0 deg C, 1 h, 2.a) 0 deg C, 6 h, b) r.t., 16 h

2: AcOH / 3 h / Heating

With acetic acid; 1,1'-carbonyldiimidazole;
DOI:10.1021/jm00126a003