2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester

Base Information

Chemical Name:2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester
CAS No.:108303-96-4
Molecular Formula:C₁₄H₁₇NO₄
Molecular Weight:263.293
Hs Code.:

Synonyms:2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester

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Chemical Property of 2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester

There total 2 articles about 2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 57402-97-8
N-<(trimethylsilyl)methyl>benzaldimine

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 108303-96-4
2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; N,N-dimethyl-formamide; for 36h; Ambient temperature;
DOI:10.1246/bcsj.59.2537

Reference yield:

: 100-52-7
benzaldehyde

: 108303-96-4
2-({[1-Phenyl-meth-(E)-ylidene]-amino}-methyl)-succinic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent

2: 98 percent / water, tetrabutylammonium fluoride / dimethylformamide; tetrahydrofuran / 36 h / Ambient temperature

With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.59.2537