C₂₅H₃₀N₂OSi

Base Information

Chemical Name:C₂₅H₃₀N₂OSi
CAS No.:1379526-12-1
Molecular Formula:C₂₅H₃₀N₂OSi
Molecular Weight:402.611
Hs Code.:

C<sub>25</sub>H<sub>30</sub>N<sub>2</sub>OSi

Synonyms:C₂₅H₃₀N₂OSi

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Chemical Property of C₂₅H₃₀N₂OSi

Chemical Property:

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Technology Process of C₂₅H₃₀N₂OSi

There total 5 articles about C₂₅H₃₀N₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1379526-11-0
C₂₃H₂₆N₂O₂Si

: 1530-32-1
ethyltriphenylphosphonium bromide

: 1379526-17-6
C₂₅H₃₀N₂OSi

: 1379526-12-1
C₂₅H₃₀N₂OSi

Guidance literature:: ethyltriphenylphosphonium bromide; With lithium hexamethyldisilazane; In diethyl ether; at 24 ℃; for 1h; Inert atmosphere; Sealed tube;

C₂₃H₂₆N₂O₂Si; In diethyl ether; at 24 ℃; for 12h; Inert atmosphere;

Reference yield:

: 3839-31-4
dimethyl(phenyl)silyl lithium

: 1379526-17-6
C₂₅H₃₀N₂OSi

: 1379526-12-1
C₂₅H₃₀N₂OSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

1.2: 3.08 h / -78 - -23 °C / Inert atmosphere

1.3: 1.5 h / -78 - -23 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / toluene / 0.25 h / -78 - 0 °C / Inert atmosphere

2.2: 0.03 h / -78 °C / Inert atmosphere

2.3: 0.5 h / -78 - 24 °C / pH 7 / Sodium phosphate buffer; Inert atmosphere

3.1: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 12 h / 110 °C / Inert atmosphere; Sealed tube

4.1: lithium hexamethyldisilazane / diethyl ether / 1 h / 24 °C / Inert atmosphere; Sealed tube

4.2: 12 h / 24 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium hexamethyldisilazane; sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; toluene;

Reference yield:

: 156094-64-3
2-(bromomethyl)-3-bromo-6-methoxypyridine

: 1379526-17-6
C₂₅H₃₀N₂OSi

: 1379526-12-1
C₂₅H₃₀N₂OSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

1.2: 3.08 h / -78 - -23 °C / Inert atmosphere

1.3: 1.5 h / -78 - -23 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / toluene / 0.25 h / -78 - 0 °C / Inert atmosphere

2.2: 0.03 h / -78 °C / Inert atmosphere

2.3: 0.5 h / -78 - 24 °C / pH 7 / Sodium phosphate buffer; Inert atmosphere

3.1: sodium t-butanolate / bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 12 h / 110 °C / Inert atmosphere; Sealed tube

4.1: lithium hexamethyldisilazane / diethyl ether / 1 h / 24 °C / Inert atmosphere; Sealed tube

4.2: 12 h / 24 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide; lithium hexamethyldisilazane; sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; toluene;