Technology Process of C30H42N2O5
There total 4 articles about C30H42N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Alloc-NH-(CH2)2-C6H4-CHO; tert-butyl (S)-3-(4-(tert-butoxy)phenyl)-2-aminopropanoate;
With
triethylamine;
In
methanol;
at 20 ℃;
for 1h;
Molecular sieve;
With
sodium cyanoborohydride;
In
methanol;
at 0 - 20 ℃;
Molecular sieve;
With
potassium hydrogensulfate; sodium chloride;
In
water; ethyl acetate;
DOI:10.1002/psc.1256
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
1.2: Saturated solution
2.1: triethylamine / methanol / 1 h / 20 °C / Molecular sieve
2.2: 0 - 20 °C / Molecular sieve
With
lithium aluminium tetrahydride; triethylamine;
In
tetrahydrofuran; methanol;
DOI:10.1002/psc.1256
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2.2: Saturated solution
3.1: triethylamine / methanol / 1 h / 20 °C / Molecular sieve
3.2: 0 - 20 °C / Molecular sieve
With
lithium aluminium tetrahydride; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/psc.1256
