tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

Base Information

Chemical Name:tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate
CAS No.:1448675-02-2
Molecular Formula:C₁₅H₂₃N₃O₅
Molecular Weight:325.365
Hs Code.:

Synonyms:tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

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Chemical Property of tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

Chemical Property:

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Technology Process of tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

There total 4 articles about tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1448675-01-1
3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

: 1448675-02-2
tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

Guidance literature:: With potassium carbonate; In methanol; for 1h; Cooling;

Reference yield:

: 1448674-98-3
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-{[tert-butyl(dimethyl)silyl]oxy}propyl acetate

: 1448675-02-2
tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Cooling

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C

3: hydrazine hydrate / ethanol / 5 h / 20 °C / Cooling

4: potassium carbonate / methanol / 1 h / Cooling

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; potassium carbonate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; ethanol;

Reference yield:

: 1448674-99-4
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

: 1448675-02-2
tert-butyl [(4-{[1-(aminooxy)-3-hydroxypropan-2-yl]oxy}phenyl)(imino)methyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C

2: hydrazine hydrate / ethanol / 5 h / 20 °C / Cooling

3: potassium carbonate / methanol / 1 h / Cooling

With di-isopropyl azodicarboxylate; potassium carbonate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; ethanol;