2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

Base Information

Chemical Name:2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate
CAS No.:1448674-99-4
Molecular Formula:C₁₇H₂₄N₂O₆
Molecular Weight:352.387
Hs Code.:

Synonyms:2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

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Chemical Property of 2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

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Technology Process of 2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

There total 3 articles about 2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1448674-98-3
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-{[tert-butyl(dimethyl)silyl]oxy}propyl acetate

: 1448674-99-4
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h; Cooling;

Reference yield:

: 93713-40-7
Glycerin-monoacetat

: 1448674-99-4
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Cooling

With dmap; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1448674-97-2
3-{[tert-butyl(dimethyl)silyl]oxy}-2-hydroxypropyl acetate

: 1448674-99-4
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-hydroxypropyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Cooling

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran;