3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

Base Information

Chemical Name:3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate
CAS No.:1448675-01-1
Molecular Formula:C₁₇H₂₅N₃O₆
Molecular Weight:367.402
Hs Code.:

Synonyms:3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

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Chemical Property of 3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

Chemical Property:

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Technology Process of 3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

There total 5 articles about 3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1448675-00-0
2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}-3-[(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)oxy]propyl acetate

: 1448675-01-1
3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

Guidance literature:: With hydrazine hydrate; In ethanol; at 20 ℃; for 5h; Cooling;

Reference yield:

: 93713-40-7
Glycerin-monoacetat

: 1448675-01-1
3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; triethylamine / dichloromethane / 20 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Cooling

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C

5: hydrazine hydrate / ethanol / 5 h / 20 °C / Cooling

With dmap; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; hydrazine hydrate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 1448674-97-2
3-{[tert-butyl(dimethyl)silyl]oxy}-2-hydroxypropyl acetate

: 1448675-01-1
3-(aminooxy)-2-{4-[N-(tert-butoxycarbonyl)carbamimidoyl]phenoxy}propyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 16 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Cooling

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 20 °C

4: hydrazine hydrate / ethanol / 5 h / 20 °C / Cooling

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; ethanol;