(2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

Base Information

Chemical Name:(2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester
CAS No.:1447810-81-2
Molecular Formula:C₂₅H₂₈INO₃
Molecular Weight:517.407
Hs Code.:

Synonyms:(2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

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Chemical Property of (2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

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Technology Process of (2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

There total 3 articles about (2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 609-67-6
2-Iodobenzoyl chloride

: 1447810-72-1
2-aminobenzoic acid undec-10-yn-1-yl ester

: 1447810-81-2
(2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c3ob41020j

Reference yield:

: 2774-84-7
undec-10-yn-1-ol

: 1447810-81-2
(2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / N,N-dimethyl-formamide / 24 h / 60 °C

2: triethylamine / dichloromethane / 0 - 20 °C

With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41020j

Reference yield:

: 118-48-9
isatoic anhydride

: 1447810-81-2
(2-iodobenzene)amidobenzoic acid undec-10-yn-1-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / N,N-dimethyl-formamide / 24 h / 60 °C

2: triethylamine / dichloromethane / 0 - 20 °C

With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41020j