(Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

Base Information

Chemical Name:(Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate
CAS No.:862549-30-2
Molecular Formula:C₂₅H₃₈O₇S
Molecular Weight:482.639
Hs Code.:

Synonyms:(Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

Suppliers and Price of (Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

There total 2 articles about (Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 862549-26-6
(Z)-5-(hydroxymethyl)-5-[(4-methoxyphenoxy)methyl]-3-[5-methyl-3-(2-methylpropyl)hexylidene]-4,5-dihydrofuran-2-one

: 124-63-0
methanesulfonyl chloride

: 862549-30-2
(Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 0.166667h;
DOI:10.1021/jm050352m

Reference yield:

: 388622-16-0
(Z)-5-[(4-methoxyphenoxy)methyl]-3-[5-methyl-3-(2-methylpropyl)hexylidene]-5-[(phenylmethoxy)methyl]-4,5-dihydrofuran-2-one

: 862549-30-2
(Z)-{2-[(4-methoxyphenoxy)methyl]-4-[5-methyl-3-(2-methylpropyl)hexylidene]-5-oxo-2-2,3-dihydrofuryl}methyl methylsulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / BCl₃ / CH₂Cl₂ / 0.33 h / -78 °C

2: 100 percent / triethylamine / CH₂Cl₂ / 0.17 h / 0 - 20 °C

With boron trichloride; triethylamine; In dichloromethane;
DOI:10.1021/jm050352m