Technology Process of C33H43NO9
There total 6 articles about C33H43NO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C31H36O10; N,N-dimethylammonium chloride;
With
sodium acetate;
In
ethyl acetate;
at 0 - 15 ℃;
Industry scale;
With
sodium tris(acetoxy)borohydride;
In
ethyl acetate;
at 0 - 40 ℃;
With
potassium hydrogencarbonate;
In
water; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dmap; pyridine; trifluorormethanesulfonic acid / 0 - 10 °C / Inert atmosphere
2.1: triethylamine hydrochloride / camphor-10-sulfonic acid / ethyl acetate / 15 - 25 °C / Industry scale
3.1: pyridine; water; potassium permanganate / 25 - 55 °C / Industry scale
4.1: sodium periodate; pyridine / acetonitrile; water / 2 h / 15 - 50 °C / Industry scale
5.1: sodium acetate / ethyl acetate / 0 - 15 °C / Industry scale
5.2: 0 - 40 °C
With
pyridine; dmap; potassium permanganate; sodium periodate; trifluorormethanesulfonic acid; water; sodium acetate; triethylamine hydrochloride;
camphor-10-sulfonic acid;
In
water; ethyl acetate; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: malonic acid; tetrabutylammonium borohydride / acetic acid methyl ester / 30 - 35 °C / Industry scale
2.1: dmap; pyridine; trifluorormethanesulfonic acid / 0 - 10 °C / Inert atmosphere
3.1: triethylamine hydrochloride / camphor-10-sulfonic acid / ethyl acetate / 15 - 25 °C / Industry scale
4.1: pyridine; water; potassium permanganate / 25 - 55 °C / Industry scale
5.1: sodium periodate; pyridine / acetonitrile; water / 2 h / 15 - 50 °C / Industry scale
6.1: sodium acetate / ethyl acetate / 0 - 15 °C / Industry scale
6.2: 0 - 40 °C
With
pyridine; dmap; potassium permanganate; sodium periodate; malonic acid; trifluorormethanesulfonic acid; water; sodium acetate; triethylamine hydrochloride; tetrabutylammonium borohydride;
camphor-10-sulfonic acid;
In
acetic acid methyl ester; water; ethyl acetate; acetonitrile;