(6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

Base Information

Chemical Name:(6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate
CAS No.:1253587-35-7
Molecular Formula:C₃₆H₃₈O₆
Molecular Weight:566.694
Hs Code.:

Synonyms:(6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

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Chemical Property of (6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

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Technology Process of (6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

There total 6 articles about (6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1486-53-9
4-(benzyloxy)-3-methoxybenzoic acid

: 171270-07-8
(6-Benzyloxy-3,4-dihydro-2,5,7,8-tetramethyl-2H-1-benzopyran-2-yl)methanol

: 1253587-35-7
(6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/jf102287h

Reference yield:

: 64338-22-3
benzyl 6-(benzyloxy)-2,5,7,8-tetramethylchroman-2-carboxylate

: 1253587-35-7
(6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; 2: Steglich esterification;
DOI:10.1021/jf102287h

Reference yield:

: 100-39-0
benzyl bromide

: 1253587-35-7
(6-benzyloxy-2,5,7,8-tetramethylchroman-2-yl)methyl 3-methoxy-4-benzyloxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 20 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 3: Steglich esterification;
DOI:10.1021/jf102287h