L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

Base Information

Chemical Name:L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)
CAS No.:1289648-10-7
Molecular Formula:C₁₈H₂₃N₄O₅
Molecular Weight:375.404
Hs Code.:

Synonyms:L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

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Chemical Property of L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

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Technology Process of L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

There total 5 articles about L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₆N₄O₅

: 1289648-10-7
L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

Guidance literature:: With sodium periodate; In dichloromethane; water; at 0 ℃; for 0.5h;
DOI:10.1016/j.molstruc.2010.12.024

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1289648-10-7
L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0 - 20 °C

3: methanol / 6 h / 20 °C

4: sodium periodate / dichloromethane; water / 0.5 h / 0 °C

With sodium periodate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; triethylamine; In methanol; dichloromethane; water;
DOI:10.1016/j.molstruc.2010.12.024

Reference yield:

: 1289648-09-4
L-N-p-nitrobenzoylpyrrolidin-2-ylmethanol

: 1289648-10-7
L-N-p-nitrobenzoylpyrrolidin-2-yl(4,5-dihydro-4,4,5,5-tetramethyl-3-oxido-1H-imidazol-3-ium-1-oxyl-2-yl)

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid / dichloromethane / 0 - 20 °C

2: methanol / 6 h / 20 °C

3: sodium periodate / dichloromethane; water / 0.5 h / 0 °C

With sodium periodate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; trichloroisocyanuric acid; In methanol; dichloromethane; water;
DOI:10.1016/j.molstruc.2010.12.024