2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

Base Information

Chemical Name:2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester
CAS No.:1260628-35-0
Molecular Formula:C₂₆H₃₈O₄
Molecular Weight:414.585
Hs Code.:

Synonyms:2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

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Chemical Property of 2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

Chemical Property:

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Technology Process of 2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

There total 8 articles about 2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₀O₄

: 1260628-35-0
2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

Guidance literature:: With hydrogen; 5% Pd(II)/C(eggshell); In ethyl acetate; for 3h; under 2250.23 Torr;

Reference yield:

: 22428-87-1
4,4-ethylenedioxycyclohexan-1-ol

: 1260628-35-0
2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

1.2: 0.33 h / 20 °C

2.1: hydrogenchloride; water / tetrahydrofuran / Reflux

3.1: lithium diisopropyl amide / hexane; tetrahydrofuran; ethylbenzene / 0.5 h / 0 - 5 °C

3.2: -78 - 20 °C

3.3: 3 h / 20 °C / pH 2

4.1: lithium diisopropyl amide / hexane; tetrahydrofuran; ethylbenzene / 0.83 h / -78 °C

4.2: 1 h / -78 °C

5.1: hydrogenchloride; water / acetone / 1 h / 120 °C / Microwave irradiation

6.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

7.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 3 h / 2250.23 Torr

With hydrogenchloride; water; hydrogen; sodium hydride; triethylamine; lithium diisopropyl amide; 5% Pd(II)/C(eggshell); In tetrahydrofuran; hexane; dichloromethane; ethylbenzene; ethyl acetate; acetone; mineral oil;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1260628-35-0
2,2-dimethyl-propionic acid 4-(4-hydroxy-cyclohexylmethyl)-3-oxo-2-(2.4,6-trimethyl-phenyl)-cyclopentyl ester

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate; methanol / 3 h / 5 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 20 °C

2.2: 0.33 h / 20 °C

3.1: hydrogenchloride; water / tetrahydrofuran / Reflux

4.1: lithium diisopropyl amide / hexane; tetrahydrofuran; ethylbenzene / 0.5 h / 0 - 5 °C

4.2: -78 - 20 °C

4.3: 3 h / 20 °C / pH 2

5.1: lithium diisopropyl amide / hexane; tetrahydrofuran; ethylbenzene / 0.83 h / -78 °C

5.2: 1 h / -78 °C

6.1: hydrogenchloride; water / acetone / 1 h / 120 °C / Microwave irradiation

7.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

8.1: hydrogen / 5% Pd(II)/C(eggshell) / ethyl acetate / 3 h / 2250.23 Torr

With hydrogenchloride; methanol; sodium tetrahydroborate; water; hydrogen; sodium hydride; triethylamine; lithium diisopropyl amide; 5% Pd(II)/C(eggshell); In tetrahydrofuran; hexane; dichloromethane; ethylbenzene; ethyl acetate; acetone; mineral oil;