ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate

Base Information

Chemical Name:ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate
CAS No.:159029-72-8
Molecular Formula:C₁₇H₂₁NO₄
Molecular Weight:303.358
Hs Code.:

Synonyms:ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate

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Chemical Property of ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate

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Technology Process of ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate

There total 3 articles about ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7154-66-7
2-bromobenzoic acid chloride

: 159029-72-8
ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 64 h / 0 - 5 °C

2: 1.) NaH, 2.) BuLi

With n-butyllithium; sodium hydride; triethylamine; In dichloromethane;
DOI:10.3987/COM-94-6750

Reference yield:

: 88-65-3
2-bromobenzoic-acid

: 159029-72-8
ethyl 2-cyclohexyl-2,3-dihydro-1-hydroxy-3-oxo-1H-isoindole-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride, dimethylformamide / CH₂Cl₂ / 1 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 64 h / 0 - 5 °C

3: 1.) NaH, 2.) BuLi

With n-butyllithium; oxalyl dichloride; sodium hydride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.3987/COM-94-6750