(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

Base Information

Chemical Name:(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate
CAS No.:1300019-43-5
Molecular Formula:C₁₉H₁₇ClN₂O₃S
Molecular Weight:388.875
Hs Code.:

Synonyms:(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

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Chemical Property of (S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

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Technology Process of (S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

There total 14 articles about (S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1300019-46-8
(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

: 1300019-43-5
(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

Guidance literature:: With tetraphosphorus decasulfide; sodium carbonate; In 1,2-dichloro-ethane; at 70 ℃; for 2h;

Reference yield:

: 1300019-48-0
methyl N¹-[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]-N²-{[(9H-fluoren-9-ylmethyl)oxy]carbonyl}-L-α-asparaginate

: 1300019-43-5
(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 24 h / Reflux

1.2: 2 h / 60 °C

2.1: tetraphosphorus decasulfide; sodium carbonate / 1,2-dichloro-ethane / 2 h / 70 °C

With tetraphosphorus decasulfide; sodium carbonate; triethylamine; In dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 596095-91-9
methyl (3S)-4-chloro-3-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-4-oxobutanoate

: 1300019-43-5
(S)-methyl 2-(5-(4-chlorophenyl)-7-methoxy-2-thioxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloroform / 1 h / 60 °C

2.1: triethylamine / dichloromethane / 24 h / Reflux

2.2: 2 h / 60 °C

3.1: tetraphosphorus decasulfide; sodium carbonate / 1,2-dichloro-ethane / 2 h / 70 °C

With tetraphosphorus decasulfide; sodium carbonate; triethylamine; In dichloromethane; chloroform; 1,2-dichloro-ethane;