Technology Process of C30H31NO9
There total 23 articles about C30H31NO9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C25H25NO7; di-tert-butyl dicarbonate;
With
ytterbium(III) triflate;
In
dichloromethane;
at 0 ℃;
for 48h;
With
ortho-iodoxybenzoic acid;
In
dimethyl sulfoxide;
at 25 ℃;
for 20h;
DOI:10.1021/ja063304f
- Guidance literature:
-
With
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
dimethyl sulfoxide;
at 25 ℃;
for 20h;
Inert atmosphere;
DOI:10.1002/chem.200701998
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 75 percent / Cs2CO3 / acetonitrile / 20 h / 25 °C
2.1: AgOTf / CH2Cl2 / 1 h / 25 °C
2.2: 77 percent / TBAT / CH2Cl2 / 20 h / -45 - 25 °C
3.1: 74 percent / samarium diiodide; HMPA / 2-methyl-propan-2-ol / 3 h / -78 - -45 °C
4.1: 99 percent / Schwartz's reagent / tetrahydrofuran / 16 h / Heating
5.1: 86 percent / KHMDS / tetrahydrofuran / 1 h / 0 °C
6.1: 99 percent / HCl; methanol / 16 h / 25 °C
7.1: Yb(OTf)3*xH2O / CH2Cl2 / 48 h / 0 °C
7.2: 50 percent / ortho-iodoxybenzoic acid / dimethylsulfoxide / 20 h / 25 °C
With
hydrogenchloride; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; Schwartz's reagent; silver trifluoromethanesulfonate; potassium hexamethylsilazane; caesium carbonate; ytterbium(III) triflate;
In
tetrahydrofuran; dichloromethane; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ja063304f
