3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

Base Information

Chemical Name:3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene
CAS No.:1395225-45-2
Molecular Formula:C₃₆H₃₆N₂O₆
Molecular Weight:592.692
Hs Code.:

Synonyms:3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

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Chemical Property of 3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

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Technology Process of 3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

There total 2 articles about 3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 13156-92-8
N-(furan-2-ylmethyl)-2-hydroxybenzamide

: 35168-64-0
1,4-bis(bromomethyl)-2,3,5,6-tetramethylbenzene

: 1395225-45-2
3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

Guidance literature:: N-(furan-2-ylmethyl)-2-hydroxybenzamide; With potassium carbonate; In acetone; at 20 ℃; for 0.5h;

1,4-bis(bromomethyl)-2,3,5,6-tetramethylbenzene; In acetone; for 24.5h; Reflux;
DOI:10.1016/j.ica.2012.04.007

Reference yield:

: 95-93-2
1,2,4,5-tetramethylbenzene

: 1395225-45-2
3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen bromide; acetic acid

2.1: potassium carbonate / acetone / 0.5 h / 20 °C

2.2: 24.5 h / Reflux

With hydrogen bromide; potassium carbonate; acetic acid; In acetone;
DOI:10.1016/j.ica.2012.04.007

Reference yield: 70.0%

: gadolinium(III) nitrate pentahydrate

: 1395225-45-2
3,6-bis{[(2'-furfurylaminoformyl)phenoxyl]methyl}-1,2,4,5-tetramethylbenzene

: [Gd₂(3,6-bis[[(2'-furfurylaminoformyl)phenoxyl]methyl]-1,2,4,5-tetramethylbenzene)3(NO₃)6]

Guidance literature:: In chloroform; ethyl acetate; ethyl acetate soln. of metal nitrate added to CHCl3 soln. of ligand (2:3molar ratio), mixt. stirred overnight at room temp.; ppt. filtered off, washed (EtOAc, CHCl3), dried, elem. anal.;
DOI:10.1016/j.ica.2012.04.007