6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol

Base Information

• Chemical Name: 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol
• CAS No.: 152980-15-9
• Molecular Formula: C₃₇H₅₂O₆Si
• Molecular Weight: 620.902

Synonyms:6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol

Chemical Property of 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol

Chemical Property:

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Technology Process of 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol

There total 2 articles about 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1H-imidazole (288-32-4) + Idebenone (58186-27-9) + acetyl chloride (75-36-5) + tert-butylchlorodiphenylsilane (58479-61-1) → 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol (152980-15-9)

Guidance literature:

With pyridine; sodium dithionite; In dichloromethane; water;

Reference yield:

1H-imidazole (288-32-4) + Idebenone (58186-27-9) + tert-butylchlorodiphenylsilane (58479-61-1) → 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol (152980-15-9)

Guidance literature:

With pyridine; sodium dithionite; In dichloromethane; water;

Reference yield:

boron trifluoride diethyl ether + 6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenol (152980-15-9) + methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucopyranuronate (92420-89-8) → methyl 1-O-[6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenyl]-2,3,4-tri-O-acetyl-β-D-glucopyranosiduronate (153010-30-1)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water;

upstream raw materials:

1H-imidazole

Idebenone

acetyl chloride

tert-butylchlorodiphenylsilane

Downstream raw materials:

1-Acetoxy-6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylbenzene

1-O-[2,3-Dimethoxy-4-hydroxy-6-(10-hydroxydecyl)-5-methylphenyl]-β-D-glucopyranoside

methyl 1-O-[6-(10-acetoxydecyl)-4-tert-butyldiphenylsilyloxy-2,3-dimethoxy-5-methylphenyl]-2,3,4-tri-O-acetyl-β-D-glucopyranosiduronate

Sodium 1-O-[4-hydroxy-6-(10-hydroxydecyl)-2,3-dimethoxy-5-methylphenyl]-β-D-glucopyranosiduronate

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