trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

Base Information

Chemical Name:trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate
CAS No.:702639-14-3
Molecular Formula:C₂₂H₃₃O₃PSi₂
Molecular Weight:432.647
Hs Code.:

Synonyms:trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

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Chemical Property of trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

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Technology Process of trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

There total 3 articles about trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 100-52-7
benzaldehyde

: 702639-11-0
bis(trimethylsilyl) 2,3-dihydro-1H-inden-2-ylphosphonite

: 702639-14-3
trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

Guidance literature:: In dichloromethane; at 10 ℃;
DOI:10.1023/B:RUGC.0000016042.81486.cd

Reference yield:

: 95-13-6
1-indene

: 702639-14-3
trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / azobis(isobutyronitrile) / 1 h / 100 - 120 °C

2: 83 percent / CH₂Cl₂ / 10 °C

With 2,2'-azobis(isobutyronitrile); In dichloromethane;
DOI:10.1023/B:RUGC.0000016042.81486.cd

Reference yield:

: 95-13-6
1-indene

: 702639-14-3
trimethylsilyl 2,3-dihydro-1H-inden-2-yl[phenyl(trimethylsiloxy)methyl]phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile) / 1 h / 100 - 120 °C / Inert atmosphere

2: dichloromethane / 10 °C / Inert atmosphere

With 2,2'-azobis(isobutyronitrile); In dichloromethane;
DOI:10.1002/hc.21419