N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide

Base Information

• Chemical Name: N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide
• CAS No.: 127616-57-3
• Molecular Formula: C₃₀H₄₀N₄S₂
• Molecular Weight: 520.806

Synonyms:N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide

Chemical Property of N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide

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Technology Process of N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide

There total 9 articles about N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

7-azido-2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene (127204-57-3) → 2,4-di-tert-butyl-6-cyanoaniline (17582-88-6) + N,N'-bis(2,4-di-tert-butyl-6-cyanophenyl)sulfur diimide (127204-58-4) + N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide (127616-57-3)

Guidance literature:

In ethanol; at 0 ℃; for 0.75h; Irradiation;

DOI:10.1021/ja00031a043

Reference yield: 30.0%

7-azido-2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene (127204-57-3) → 2,4-di-tert-butyl-6-cyanoaniline (17582-88-6) + 2,4-di-tert-butyl-6-cyano-N-sulfinylaniline (127616-60-8) + 2,4-di-tert-butyl-6-cyano-7,8,9-oxathiazabicyclo<4.3.0>nona-2,4,9-triene 8-oxide (127616-61-9) + N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide (127616-57-3)

Guidance literature:

With oxygen; In hexane; at 40 ℃; for 6h; Further byproducts given;

DOI:10.1246/cl.1989.2087

Reference yield: 14.0%

7-azido-2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene (127204-57-3) → 2,4-di-tert-butyl-6-cyanoaniline (17582-88-6) + 2,4-di-tert-butyl-6-cyano-7,8,9-oxathiazabicyclo<4.3.0>nona-2,4,9-triene 8-oxide (127616-61-9) + N,N'-bis(2,4-di-tert-butyl-6-cyanophenyl)sulfur diimide (127204-58-4) + N-(2,4-di-tert-butyl-6-cyanophenyl)-N'-(2',4'-di-tert-butyl-8',9'-thiazabicyclo<4.3.0>nona-2',4',6',9'-tetraen-7'-yl)sulfur diimide (127616-57-3)

Guidance literature:

With oxygen; In hexane; at 40 ℃; for 5h; Further byproducts given;

DOI:10.1021/ja00031a043

upstream raw materials:

styrenesulfide

7-azido-2,4-di-tert-butyl-8,9-thiazabicyclo<4.3.0>nona-2,4,6,9-tetraene

2-Diazo-1,1,3,3-tetramethylcyclopentane

2,3-dimethyl-buta-1,3-diene

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