6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

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Chemical Name:6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide
CAS No.:1387626-94-9
Molecular Formula:C₂₄H₂₃BClN₅OS
Molecular Weight:475.81
Hs Code.:

Synonyms:6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

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Chemical Property of 6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

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Technology Process of 6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

There total 3 articles about 6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 742105-63-1
2-chloro-10-((1E,3Z)-4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)buta-1,3-dien-1-yl)-10H-phenothiazine

: 1387626-94-9
6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

Guidance literature:: With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.05.065

Reference yield:

: 92-39-7
2-chlorophenothiazine

: 1387626-94-9
6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 48.33 h

2: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With dimethylsulfide borane complex; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1016/j.bmc.2012.05.065

Reference yield:

: 3-(4-methoxyphenyl)-tetrazolo[1,5-a]pyridin-4-ium tetrafluoroborate

: 1387626-94-9
6-((2-chloro-10H-phenothiazin-10-yl)methyl)-2-(4-methoxyphenyl)-5,6,7,8-tetrahydro-2H-tetrazolo[5,1-f][1,2]azaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 48.33 h

2: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

With dimethylsulfide borane complex; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1016/j.bmc.2012.05.065