1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

Base Information

Chemical Name:1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole
CAS No.:1619222-83-1
Molecular Formula:C₅₃H₃₆N₂
Molecular Weight:700.882
Hs Code.:

Synonyms:1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

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Chemical Property of 1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

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Technology Process of 1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

There total 12 articles about 1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1260865-91-5
4,4,5,5–tetramethyl–2–(4–(1,2,2–triphenylvinyl)phenyl)–1,3,2–dioxaborolane

: 1147081-43-3
2-(4-bromophenyl)-1-phenyl-1H-phenanthro- [9,10-d]imidazole

: 1619222-83-1
1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c4cc02824d

Reference yield: 62.15%

: 34699-28-0
1-(4-bromophenyl)triphenylethene

: 1228632-34-5
1-phenyl-2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-phenanthro[9,10-d]imidazole

: 1619222-83-1
1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; at 85 ℃; for 24h; Inert atmosphere;
DOI:10.1002/chem.201604923

Reference yield:

: 84-11-7
9,10-phenanthrenequinone

: 1619222-83-1
1-phenyl-2-(4’-(1,2,2-triphenylvinyl)-[1,1’-biphenyl]-4-yl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate; acetic acid / 2 h / 120 °C / Inert atmosphere

2: n-butyllithium / tetrahydrofuran / 28 h / -78 - 20 °C / Inert atmosphere

3: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 24 h / 85 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; ammonium acetate; potassium carbonate; acetic acid; In tetrahydrofuran; water; toluene; 3: |Suzuki Coupling;
DOI:10.1002/chem.201604923