(E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine

Base Information

• Chemical Name: (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine
• CAS No.: 170960-88-0
• Molecular Formula: C₂₂H₂₄N₄S
• Molecular Weight: 376.525

Synonyms:(E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine

Chemical Property of (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine

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Technology Process of (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine

There total 3 articles about (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tert-Butoxybis(dimethylamino)methane (5815-08-7) + (E)-N-<1-(4-methylthio)phenyl>ethylidene-1H-2-methyl-4-phenyl-1,3-imidazol-1-amine (170960-77-7) → (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine (170960-88-0)

Guidance literature:

In 1,2-dimethoxyethane; at 80 ℃; for 9h;

DOI:10.1080/00397919508015480

Reference yield:

4-(Methylthio)acetophenone (1778-09-2) → (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine (170960-88-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / glacial acetic acid / ethanol / 1 h / Heating

2: 96 percent / 1,2-dimethoxy-ethane / 9 h / 80 °C

With acetic acid; In 1,2-dimethoxyethane; ethanol;

DOI:10.1080/00397919508015480

Reference yield:

1-amino-2-methyl-4-phenylimidazole (39678-35-8) → (E,E)-N-<3-(dimethylamino)-1-<4-(methylthio)phenyl>-1H-2-propenylidene>-2-methyl-4-phenyl-1,3-imidazol-1-amine (170960-88-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / glacial acetic acid / ethanol / 1 h / Heating

2: 96 percent / 1,2-dimethoxy-ethane / 9 h / 80 °C

With acetic acid; In 1,2-dimethoxyethane; ethanol;

DOI:10.1080/00397919508015480

upstream raw materials:

tert-Butoxybis(dimethylamino)methane

(E)-N-<1-(4-methylthio)phenyl>ethylidene-1H-2-methyl-4-phenyl-1,3-imidazol-1-amine

4-(Methylthio)acetophenone

1-amino-2-methyl-4-phenylimidazole

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