2-chloro-4-cyanobenzaldoxime

Base Information

Chemical Name:2-chloro-4-cyanobenzaldoxime
CAS No.:914106-38-0
Molecular Formula:C₈H₅ClN₂O
Molecular Weight:180.593
Hs Code.:

Synonyms:2-chloro-4-cyanobenzaldoxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-4-cyanobenzaldoxime

Chemical Property:

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Technology Process of 2-chloro-4-cyanobenzaldoxime

There total 3 articles about 2-chloro-4-cyanobenzaldoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58588-64-0
3-chloro-4-formyl-benzonitrile

: 914106-38-0
2-chloro-4-cyanobenzaldoxime

Guidance literature:: With hydroxylamine hydrochloride; In ethanol;
DOI:10.1021/jm0612867

Reference yield:

: 21924-83-4
4-(bromomethyl)-3-chlorobenzonitrile

: 914106-38-0
2-chloro-4-cyanobenzaldoxime

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / NaOEt; 2-nitropropane

2: 92 percent / hydroxylamine hydrochloride / aq. ethanol

With 2-nitropropane; hydroxylamine hydrochloride; sodium ethanolate; In ethanol;
DOI:10.1021/jm0612867

Reference yield:

: 21423-81-4
3-chloro-4-methylbenzonitrile

: 914106-38-0
2-chloro-4-cyanobenzaldoxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-bromosuccinimide; benzoyl peroxide / CCl₄

1.2: diethyl phosphite; iPr₂NEt / tetrahydrofuran

2.1: 89 percent / NaOEt; 2-nitropropane

3.1: 92 percent / hydroxylamine hydrochloride / aq. ethanol

With N-Bromosuccinimide; 2-nitropropane; hydroxylamine hydrochloride; sodium ethanolate; dibenzoyl peroxide; In tetrachloromethane; ethanol;
DOI:10.1021/jm0612867