({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Base Information

Chemical Name:({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid
CAS No.:1337864-00-2
Molecular Formula:C₆₉H₇₄B₂N₈O₉
Molecular Weight:1181.02
Hs Code.:

({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Synonyms:({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

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Chemical Property of ({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

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Technology Process of ({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

There total 5 articles about ({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1337863-99-6
tert-butyl {3-[4({2,5-bis[methyl({10-[(methylamino)methyl]-anthracene-9-yl}methyl)carbamoyl]phenoxy}methyl)-1H-1,2,3-triazol-1-yl]propyl}-carbamate

: 166821-88-1
5,5-dimethyl-2-(2-bromomethylphenyl)-1,3,2-dioxaborinane

: 1337864-00-2
({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Guidance literature:: With potassium carbonate; sodium iodide; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere; Darkness;
DOI:10.1039/c1cc11814e

Reference yield:

: 181022-08-2
2-prop-2-ynyloxy-terephthalic acid dimethyl ester

: 1337864-00-2
({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / methanol / 3 h / Reflux

2: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Darkness

4: copper(l) iodide; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.5 h / 80 °C / Microwave irradiation; Inert atmosphere

5: potassium carbonate; sodium iodide / acetonitrile / 16 h / 20 °C / Inert atmosphere; Darkness

With dmap; copper(l) iodide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium iodide; sodium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c1cc11814e

Reference yield:

: 181022-09-3
2-(prop-2-yn-1-yloxy)terephthalic acid

: 1337864-00-2
({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Darkness

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / dimethyl sulfoxide / 0.5 h / 80 °C / Microwave irradiation; Inert atmosphere

4: potassium carbonate; sodium iodide / acetonitrile / 16 h / 20 °C / Inert atmosphere; Darkness

With dmap; copper(l) iodide; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium iodide; In dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c1cc11814e