({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Base Information

• Chemical Name: ({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid
• CAS No.: 1337864-01-3
• Molecular Formula: C₆₄H₆₆B₂N₈O₇
• Molecular Weight: 1080.9

Synonyms:({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Chemical Property of ({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Chemical Property:

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Technology Process of ({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

There total 1 articles about ({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid (1337864-00-2) → ({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid (1337864-01-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h; Darkness; Inert atmosphere;

DOI:10.1039/c1cc11814e

Reference yield: 80.0%

({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid (1337864-01-3) + C32H32BF2N5O6 → C92H93B3F2N12O10

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1016/j.bmcl.2013.09.063

Reference yield: 36.0%

2,5-dioxopyrrolidin-1-yl 3-[({3-[5-(benzylamino)-5-oxopent-1-yn-1-yl]-4-methoxyphenyl}bis{4-methoxyphenyl}methyl)thio]propanoate (1337864-02-4) + ({[({[({2-[(1-{3-aminopropyl}-1H-1,2,3-triazol-4-yl)methoxy]-terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis-(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid (1337864-01-3) → [({[({[({2-[(1-{3-[({3-[5-(benzylamino)-5-oxopent-1-yn-1-yl]-4-methoxyphenyl}bis(4-methoxyphenyl)methyl)thio]propanamido}prop-3-yl)-1H-1,2,3-triazol-4-yl]methoxy}terephthaloyl)bis(methylazanediyl)]bis(methylene)}bis(anthracene-10,9-diyl))bis(methylene)]bis(methylazanediyl)}bis(methylene))bis(2,1-phenylene)]-diboronic acid

Guidance literature:

With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

upstream raw materials:

({[({[({2-[(1-{3-[(tert-butoxycarbonyl)amino]propyl}-1H-1,2,3-triazol-4-yl)methoxy]terephthaloyl}bis(methylazanediyl))bis(methylene)]bis(anthracene-10,9-diyl)}bis(methylene))bis(methylazanediyl)]bis(methylene)}bis(2,1-phenylene))-diboronic acid

Downstream raw materials:

C₁₀₁H₁₀₁B₂N₉O₁₂S

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