methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

Base Information

Chemical Name:methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate
CAS No.:339354-72-2
Molecular Formula:C₁₈H₁₈N₂O₂S₂
Molecular Weight:358.485
Hs Code.:

Synonyms:methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

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Chemical Property of methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

Chemical Property:

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Technology Process of methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

There total 4 articles about methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134469-07-1
Benzimidazol-2-thiol

: 339354-71-1
methyl 2-{[3-(chloromethyl)-2-methylphenyl]sulfanyl}acetate

: 339354-72-2
methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

Guidance literature:: With sodium hydroxide; In methanol; water; at 20 ℃; for 6h;
DOI:10.1021/jm020868v

Reference yield:

: 52130-17-3
3-amino-2-methylbenzoic acid

: 339354-72-2
methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: HCl; NaNO₂ / H₂O / 0 °C

1.2: Na₂CO₃ / methanol; H₂O / 0.75 h / 60 - 70 °C / pH 5 - 6

2.1: 5 g / BH₃*THF / 1 h / 0 °C

3.1: thionyl chloride / CH₂Cl₂ / 4 h / 20 °C

4.1: 4.2 g / NaOH / H₂O; methanol / 6 h / 20 °C

With hydrogenchloride; sodium hydroxide; thionyl chloride; borane-THF; sodium nitrite; In methanol; dichloromethane; water;
DOI:10.1021/jm020868v

Reference yield:

: 339354-70-0
methyl 2-{[3-(hydroxymethyl)-2-methylphenyl]sulfanyl}acetate

: 339354-72-2
methyl 2-({3-[(1H-benzimidazol-2-ylsulfanyl)methyl]-2-methylphenyl}sulfanyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / CH₂Cl₂ / 4 h / 20 °C

2: 4.2 g / NaOH / H₂O; methanol / 6 h / 20 °C

With sodium hydroxide; thionyl chloride; In methanol; dichloromethane; water;
DOI:10.1021/jm020868v