(S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

Base Information

Chemical Name:(S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate
CAS No.:1234550-77-6
Molecular Formula:C₁₇H₂₅NO₆
Molecular Weight:339.389
Hs Code.:

Synonyms:(S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

Chemical Property:

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Technology Process of (S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

There total 7 articles about (S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1177255-28-5
(S)-methyl-2-acetamido-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

: 1234550-77-6
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

Guidance literature:: (S)-methyl-2-acetamido-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate; With thionyl chloride; In chloroform; at 80 ℃;

di-tert-butyl dicarbonate; With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetlet.2018.07.003

Reference yield: 91.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1308253-76-0
C₁₂H₁₇NO₄

: 1234550-77-6
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1002/jhet.609

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₀H₂₃NO₆

: 1234550-77-6
(S)-methyl 2-(tert-butoxycarbonylamino)-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

Guidance literature:: With 10% palladium on activated carbon; hydrogen; In methanol; at 20 ℃; for 10h; under 760.051 Torr;
DOI:10.1021/jo100788j