[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Base Information

Chemical Name:[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate
CAS No.:1383577-57-8
Molecular Formula:C₄₀H₃₀N₁₀O₈
Molecular Weight:778.74
Hs Code.:

[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Synonyms:[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

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Chemical Property of [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

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Technology Process of [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

There total 6 articles about [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1383577-56-7
2-(4-[((2-[4-(([2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)phenyl]carbonyloxy)methyl)-1H-1,2,3-triazol-1-yl]phenyl)carbonyloxy)methyl]-1H-1,2,3-triazol-1-yl)benzoic acid

: 106-96-7
propargyl bromide

: 1383577-57-8
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: 2-(4-[((2-[4-(([2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)phenyl]carbonyloxy)methyl)-1H-1,2,3-triazol-1-yl]phenyl)carbonyloxy)methyl]-1H-1,2,3-triazol-1-yl)benzoic acid; With potassium carbonate; In N,N-dimethyl-formamide; for 0.0833333h; Reflux;

propargyl bromide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1055/s-0031-1290760

Reference yield:

: 1383577-47-6
2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

: 1383577-57-8
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / water; acetone

1.2: 0.08 h / 0 °C

1.3: 0.5 h / 0 - 20 °C

2.1: copper(II) sulfate; ascorbic acid / water; N,N-dimethyl-formamide / 0.5 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

3.2: 20 °C

With hydrogenchloride; potassium carbonate; copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1055/s-0031-1290760

Reference yield:

: 31162-13-7
2-azidobenzoic acid

: 1383577-57-8
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(II) sulfate; ascorbic acid / water; butan-1-ol / 1 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

2.2: 20 °C

3.1: copper(II) sulfate; ascorbic acid / water; N,N-dimethyl-formamide / 0.5 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

4.2: 20 °C

With potassium carbonate; copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1055/s-0031-1290760