[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

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Chemical Name:[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate
CAS No.:1383577-58-9
Molecular Formula:C₄₀H₂₈N₁₂O₈
Molecular Weight:804.738
Hs Code.:

[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Synonyms:[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

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Chemical Property of [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

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Technology Process of [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

There total 7 articles about [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1383577-57-8
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

: 1383577-58-9
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: [1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate; With hydrogenchloride; In water; acetone;

With sodium nitrite; In water; acetone; at 0 ℃; for 0.0833333h;

With sodium azide; In water; acetone; at 0 - 20 ℃; for 0.5h;
DOI:10.1055/s-0031-1290760

Reference yield:

: 1383577-47-6
2-(4-([(2-aminophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoic acid

: 1383577-58-9
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / water; acetone

1.2: 0.08 h / 0 °C

1.3: 0.5 h / 0 - 20 °C

2.1: copper(II) sulfate; ascorbic acid / water; N,N-dimethyl-formamide / 0.5 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

3.2: 20 °C

4.1: hydrogenchloride / water; acetone

4.2: 0.08 h / 0 °C

4.3: 0.5 h / 0 - 20 °C

With hydrogenchloride; potassium carbonate; copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1055/s-0031-1290760

Reference yield:

: 31162-13-7
2-azidobenzoic acid

: 1383577-58-9
[1-(2-([(1-(2-[(prop-2-yn-1-yloxy)carbonyl]phenyl)-1H-1,2,3-triazol-4-yl)methoxy]carbonyl)phenyl)-1H-1,2,3-triazol-4-yl]methyl 2-(4-([(2-azidophenyl)carbonyloxy]methyl)-1H-1,2,3-triazol-1-yl)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(II) sulfate; ascorbic acid / water; butan-1-ol / 1 h / 20 °C

2.1: hydrogenchloride / water; acetone

2.2: 0.08 h / 0 °C

2.3: 0.5 h / 0 - 20 °C

3.1: copper(II) sulfate; ascorbic acid / water; N,N-dimethyl-formamide / 0.5 h / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux

4.2: 20 °C

5.1: hydrogenchloride / water; acetone

5.2: 0.08 h / 0 °C

5.3: 0.5 h / 0 - 20 °C

With hydrogenchloride; potassium carbonate; copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide; acetone; butan-1-ol;
DOI:10.1055/s-0031-1290760