N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

Base Information

Chemical Name:N,N'-dinitrostyphnyl bis-3-alaninoyl chloride
CAS No.:321567-72-0
Molecular Formula:C₁₂H₉Cl₂N₇O₁₂
Molecular Weight:514.149
Hs Code.:

Synonyms:N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

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Technology Process of N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

There total 3 articles about N,N'-dinitrostyphnyl bis-3-alaninoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 321567-70-8
N,N'-dinitrostyphnyl-bis-β-alanine

: 321567-72-0
N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

Guidance literature:: With phosphorus pentachloride; In benzene; at 80 ℃; for 4h;

Reference yield:

: 1630-09-7
2,4-dichloro-1,3,5-trinitrobenzene

: 321567-72-0
N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / sodium carbonate / ethanol; H₂O / 0.5 h / 60 °C

2: 85 percent / conc. H₂SO₄; fuming nitric acid / 4 h / 50 °C

3: 74 percent / PCl₅ / benzene / 4 h / 80 °C

With phosphorus pentachloride; sulfuric acid; nitric acid; sodium carbonate; In ethanol; water; benzene;

Reference yield:

: 321567-68-4
styphnylbis-β-alanine

: 321567-72-0
N,N'-dinitrostyphnyl bis-3-alaninoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / conc. H₂SO₄; fuming nitric acid / 4 h / 50 °C

2: 74 percent / PCl₅ / benzene / 4 h / 80 °C

With phosphorus pentachloride; sulfuric acid; nitric acid; In benzene;