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1,3-DICHLORO-2,4,6-TRINITROBENZENE is a chemical with a specific purpose. Lookchem provides you with multiple data and supplier information of this chemical.

1630-09-7

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1630-09-7 Usage

Synthesis Reference(s)

The Journal of Organic Chemistry, 26, p. 2997, 1961 DOI: 10.1021/jo01066a613

Check Digit Verification of cas no

The CAS Registry Mumber 1630-09-7 includes 7 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 4 digits, 1,6,3 and 0 respectively; the second part has 2 digits, 0 and 9 respectively.
Calculate Digit Verification of CAS Registry Number 1630-09:
(6*1)+(5*6)+(4*3)+(3*0)+(2*0)+(1*9)=57
57 % 10 = 7
So 1630-09-7 is a valid CAS Registry Number.
InChI:InChI=1/C6HCl2N3O6/c7-4-2(9(12)13)1-3(10(14)15)5(8)6(4)11(16)17/h1H

1630-09-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 18, 2017

Revision Date: Aug 18, 2017

1.Identification

1.1 GHS Product identifier

Product name 2,4-Dichloro-1,3,5-trinitrobenzene

1.2 Other means of identification

Product number -
Other names styphnyl chloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1630-09-7 SDS

1630-09-7Relevant articles and documents

Synthesis of 1,3-bis(1,2,4-triazol-3-amino)-2,4,6-trinitrobenzene and its thermal and explosive behaviour

Agrawal,Mehilal,Prasad,Surve

, p. 583 - 585 (2000)

1,3-Bis(1,2,4-triazol-3-amino)-2,4,6-trinitrobenzene (BTATNB) has been synthesized by condensing 1,3-dichloro-2,4, 6-trinitrobenzene and 3-amino-1,2,4-triazole in dimethyl formamide (DMF) at 125 ± 2 °C. The product has been characterized by elemental analysis, Fourier transform infrared (FTIR), nuclear magnetic resonance (NMR) and mass spectrometry. The data on thermal and explosive properties indicate that BTATNB is slightly more thermally stable than 3-picrylamino-1,2,4-triazole (PATO). At the same time, it is safer towards impact and friction.

Nitroanilinodinitrobenzofuroxans - Synthesis, characterisation, thermal stability and explosive properties

Mehilal,Sikder,Salunke,Sikder

, p. 1549 - 1552 (2007/10/03)

Three new derivatives of 4,6-dinitrobenzofuroxan: 7-(4-nitrophenylamino)-4,6-dinitrobenzofuroxan, 7-(3,5-dinitrophenylamino)-4,6-dinitrobenzofuroxan and 7-(2,4,6-trinitrophenylamino)-4,6-dinitrobenzofuroxan, have been synthesised by condensing 4-nitroaniline, 3,5-dinitroaniline and 2,4,6-trinitroaniline with 7-chloro-4,6-dinitrobenzofuroxan, respectively. The characterisation of the compounds by IR, 1H-NMR, mass spectrometry and elemental analysis is described along with some of the evaluated preliminary explosive properties. The compounds were found to exhibit acceptable hazards properties. Furthermore, the thermal stability measurements indicated acceptable stability.

Chloro- and bromo-demethoxylation of methoxypolynitroaryl systems

Bellamy, Anthony J.,Hudson, P. Nick

, p. 5639 - 5642 (2007/10/03)

Various reagents for effecting halogenodemethoxylation of methoxy substituted polynitrophenyl and -biphenyl systems have been investigated, and the preferred procedures for achieving chloro- and bromo-demethoxylation in high yield have been identified.

Benzenepentamine - Its Easy Accessibility and Use in Syntheses of Pyrazinoquinoxalines

Praefcke, Klaus,Kohne, Bernd,Korinth, Frank,Psaras, Panicos,Nasielski, Jaques,et al.

, p. 617 - 622 (2007/10/02)

Benzenepentamine (6) has been rediscovered after about 60 years.A simple and very efficient synthetic route is described which yields the very sensitive, colourless 6 in methanolic solution in nearly quantitative yield.Condensations of 6 with two masked forms A and B of glyoxal conveniently lead to two types of amino-substituted pyrazinoquinoxalines, one with an angular phenanthrene-type topology (7a), or one with the linear anthracene-type structure (8a), respectively, with acceptable yields.The α-diketone benzil also reacts with 6, but less selectively, forming the corresponding tetraphenyl derivatives 7b and 8b of both these heterotricyclic ring systems.The heretofore unknown nitrobenzenepentamine (9), formed in addition to benzenehexamine in reduction reactions of 1,3,5-trinitrobenzenetriamine, has also been obtained.Based on spectroscopic data, the structures of these two multiamines have been deduced from their condensation products with α-diketones, in the case of the new pentamine 9 from its first derivatives 7c-e of pyrazinoquinoxaline.

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