N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide
CAS No.:1313872-22-8
Molecular Formula:C₂₇H₃₀N₂O₄S
Molecular Weight:478.612
Hs Code.:

Synonyms:N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

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Chemical Property of N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

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Technology Process of N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

There total 2 articles about N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1160027-97-3
(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

: 13139-86-1
4-methoxyphenyl magnesium bromide

: N-(1-(4-methoxybenzyl)-(R,R)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

: 1313872-22-8
N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: (R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide; With magnesium bromide; In dichloromethane; at -40 ℃; for 0.333333h; Inert atmosphere;

4-methoxyphenyl magnesium bromide; In dichloromethane; at -40 - 20 ℃; Inert atmosphere;

With water; ammonium chloride; In dichloromethane; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo900623c

Reference yield:

: 1160027-97-3
(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

: 7294-51-1
2,4,6-tris(4-methoxyphenyl)boroxine

: N-(1-(4-methoxybenzyl)-(R,R)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

: 1313872-22-8
N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium ethanolate; In 1,4-dioxane; ethanol; at 20 ℃; for 18h; optical yield given as %de; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol201438k