(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide
CAS No.:1160027-97-3
Molecular Formula:C₂₀H₂₂N₂O₃S
Molecular Weight:370.472
Hs Code.:

Synonyms:(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

Suppliers and Price of (R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

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Technology Process of (R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

There total 1 articles about (R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 31541-32-9
1-(4-methoxybenzyl)-1H-indole-2,3-dione

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 1160027-97-3
(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

Guidance literature:: With titanium(IV) tetraethanolate; In dichloromethane; at 20 ℃; Inert atmosphere; Reflux;
DOI:10.1021/jo900623c

Reference yield: 90.0%

: 1160027-97-3
(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

: 106-95-6
allyl bromide

: 1422181-74-5
(R)-N-((S)-3-allyl-1-(4-methoxybenzyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; zinc; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c2cc38600c

Reference yield: 53.0%

: 1160027-97-3
(R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide

: 13139-86-1
4-methoxyphenyl magnesium bromide

: N-(1-(4-methoxybenzyl)-(R,R)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

: 1313872-22-8
N-(1-(4-methoxybenzyl)-(R,S)-3-(4-methoxyphenyl)-2-oxoindolin-3-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: (R)-N-(1-(4-methoxybenzyl)-2-oxoindolin-3-ylidene)-2-methylpropane-2-sulfinamide; With magnesium bromide; In dichloromethane; at -40 ℃; for 0.333333h; Inert atmosphere;

4-methoxyphenyl magnesium bromide; In dichloromethane; at -40 - 20 ℃; Inert atmosphere;

With water; ammonium chloride; In dichloromethane; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo900623c