Technology Process of C25H17BF5N5O
There total 5 articles about C25H17BF5N5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(I) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
ethanol; water;
at 20 ℃;
DOI:10.1007/s11426-011-4452-2
- Guidance literature:
-
Multi-step reaction with 4 steps
1: chloranil
2: boron trifluoride diethyl etherate; triethylamine / toluene / Reflux
3: sodium azide / acetonitrile / 3 h / 20 °C / Darkness
4: copper(I) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / ethanol; water / 20 °C
With
sodium azide; copper(I) sulfate; boron trifluoride diethyl etherate; chloranil; sodium L-ascorbate; triethylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
ethanol; water; toluene; acetonitrile;
DOI:10.1007/s11426-011-4452-2
- Guidance literature:
-
Multi-step reaction with 6 steps
1: trifluoroacetic acid / 20 °C / Neat (no solvent)
2: N-chloro-succinimide / tetrahydrofuran / -78 °C
3: chloranil
4: boron trifluoride diethyl etherate; triethylamine / toluene / Reflux
5: sodium azide / acetonitrile / 3 h / 20 °C / Darkness
6: copper(I) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / ethanol; water / 20 °C
With
N-chloro-succinimide; sodium azide; copper(I) sulfate; boron trifluoride diethyl etherate; chloranil; sodium L-ascorbate; triethylamine; trifluoroacetic acid; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
tetrahydrofuran; ethanol; water; toluene; acetonitrile;
DOI:10.1007/s11426-011-4452-2