O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

Base Information

Chemical Name:O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate
CAS No.:577974-52-8
Molecular Formula:C₄₀H₇₁BrNO₃P
Molecular Weight:724.886
Hs Code.:

Synonyms:O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

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Technology Process of O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

There total 3 articles about O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 57-88-5
cholesterol

: 577974-45-9
O-(3-menthyl)-[N-(2-bromoethyl)-N-methyl]-amidobromophosphate

: 577974-52-8
O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

Guidance literature:: With pyridine; In 1,4-dioxane; at 80 ℃; for 26h;
DOI:10.1023/A:1022505916623

Reference yield:

: 2216-51-5
(-)-menthol

: 577974-52-8
O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / benzene / 4 h / 80 °C

2: 100 percent / bromine / CHCl₃ / 0.17 h / -30 °C

3: 48 percent / pyridine / dioxane / 26 h / 80 °C

With pyridine; bromine; In 1,4-dioxane; chloroform; benzene;
DOI:10.1023/A:1022505916623

Reference yield:

: 577974-43-7,92208-93-0
3-methyl-2-(3-menthyloxy)-1,3,2-oxaazaphospholane

: 577974-52-8
O-(3-menthyl)-O-(3-cholesteryl)-[N-(2-bromoethyl)-N-methyl]amidophosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / bromine / CHCl₃ / 0.17 h / -30 °C

2: 48 percent / pyridine / dioxane / 26 h / 80 °C

With pyridine; bromine; In 1,4-dioxane; chloroform;
DOI:10.1023/A:1022505916623