Technology Process of [(N,N-bis((6-phenyl-2-pyridyl)methyl-N-((2-pyridyl)methyl)amine)Co(ONHC(O)CH3)](ClO4)
There total 1 articles about [(N,N-bis((6-phenyl-2-pyridyl)methyl-N-((2-pyridyl)methyl)amine)Co(ONHC(O)CH3)](ClO4) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(CH3)4NOH*5H2O;
In
methanol;
soln. of Co salt in MeOH added to slurry of the amine in MeOH, stirred at ambient temp. for ca. 35 min, added to Me4NOH*5H2O in MeOH, stirred for 1 h, added to soln. of acetohydroxamic acid in MeOH, stirred for 12 h; evapd., residue dried, dissolved in CH2Cl2, filtered through Celite, filtrate evapd. to dryness, recrystd. by Et2O diffusion into a i-PrOH/MeCN soln.; elem. anal.;
DOI:10.1021/ic034810y
