t-butyl phenoxypyruvate

Base Information

• Chemical Name: t-butyl phenoxypyruvate
• CAS No.: 872526-15-3
• Molecular Formula: C₁₃H₁₆O₄
• Molecular Weight: 236.268
• Mol file: 872526-15-3.mol

Synonyms:t-butyl phenoxypyruvate

Chemical Property of t-butyl phenoxypyruvate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of t-butyl phenoxypyruvate

There total 3 articles about t-butyl phenoxypyruvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

t-butyl 2-hydroxy-3-phenoxypropioate (872526-09-5) → t-butyl phenoxypyruvate (872526-15-3)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h;

DOI:10.3987/COM-05-10504

Reference yield:

tert-butyl cis-2,3-dihydroxypropanoate (235090-36-5) → t-butyl phenoxypyruvate (872526-15-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / NaH / various solvent(s) / 43 h / 45 °C

2: 85 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With sodium hydride; Dess-Martin periodane; In dichloromethane;

DOI:10.3987/COM-05-10504

Reference yield:

phenol (108-95-2,27073-41-2) → t-butyl phenoxypyruvate (872526-15-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / NaH / various solvent(s) / 43 h / 45 °C

2: 85 percent / Dess-Martin periodinane / CH₂Cl₂ / 3 h / 20 °C

With sodium hydride; Dess-Martin periodane; In dichloromethane;

DOI:10.3987/COM-05-10504

upstream raw materials:

t-butyl 2-hydroxy-3-phenoxypropioate

tert-butyl cis-2,3-dihydroxypropanoate

phenol