Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid
CAS No.:76909-79-0
Molecular Formula:C₅₆H₅₉NO₁₁
Molecular Weight:922.085
Hs Code.:

Synonyms:Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

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Chemical Property of Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

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Technology Process of Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

There total 1 articles about Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 70209-55-1
benzyl 2-acetamido-3,6-di-O-benzyl-4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-2-deoxy-α-D-glucopyranoside

: 100-39-0
benzyl bromide

: 76909-79-0
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 0 ℃; for 3h;

Reference yield: 89.0%

: 76909-79-0
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

: 76909-80-3
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-β-D-galactopyranosyl)-α-D-glucopyranosid

Guidance literature:: With acetic acid; at 60 ℃; for 2.5h;

Reference yield:

: 76909-79-0
Benzyl-2-acetamido-3,6-di-O-benzyl-2-desoxy-4-O-(2,3-di-O-benzyl-4,6-O-benzyliden-β-D-galactopyranosyl)-α-D-glucopyranosid

: 76909-82-5
Benzyl-2-acetamido-4-O-<4-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-6-O-benzoyl-2,3-di-O-benzyl-β-D-galactopyranosyl>-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / 90percent CH₃COOH / 2.5 h / 60 °C

2: 92 percent / CH₂Cl₂; pyridine / 72 h / 0 °C

3: 1.) Ag₂CO₃, molecular sieves 4 Angstroem, 2.) AgClO₄ / 1.) CH₂Cl₂, r.t., 2.) CH₂Cl₂, 0 deg C; r.t.

With 4 A molecular sieve; silver perchlorate; acetic acid; silver carbonate; In pyridine; dichloromethane;