2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene

Base Information

• Chemical Name: 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene
• CAS No.: 88589-36-0
• Molecular Formula: C₄₁H₄₀N₂O₆S₂
• Molecular Weight: 720.91

Synonyms:2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene

Chemical Property of 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene

Chemical Property:

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Technology Process of 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene

There total 1 articles about 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C27H28N2O6S2 (72374-10-8) + benzyl bromide (100-39-0) → 2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 72h; Heating;

DOI:10.1021/jo00180a001

Reference yield: 84.0%

2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0) → 1-Benzyl-8-(benzylamino)-6,9-dimethyl-2,5-dioxo-1,2,3,4,5,6-hexahydro-1-benzazocine (88609-66-9)

Guidance literature:

With anthracene; N,N,N,N-tetraethylammonium tetrafluoroborate; ascorbic acid; In N,N-dimethyl-formamide; for 7.5h; Mechanism; Product distribution; electrolysis with Hg cathode at -1.7 to -1.9 V vs. SCE; variation of additives, reaction time;

DOI:10.1021/jo00180a001

Reference yield: 48.0%

2,5-Bis-4-(2,5-dioxo-1-methylcyclopentyl)toluene (88589-36-0) → 4-Benzyl-7-(benzylamino)-6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole (88589-38-2)

Guidance literature:

With 1,5-dimethoxynaphthalene; ascorbic acid; In tetrahydrofuran; water; for 8h; Irradiation;

DOI:10.1021/jo00180a001

upstream raw materials:

C₂₇H₂₈N₂O₆S₂

benzyl bromide

Downstream raw materials:

4-Benzyl-7--6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole

2,5-Bis-4-(1-methyl-2-oxo-4-carbomethoxybutyl)toluene

2,5-Bis-4-(1-methyl-2-oxo-4-carboethoxybutyl)toluene

4-Benzyl-7-(benzylamino)-6,8b-dimethyl-3a-hydroxy-1-oxo-1,2,3,3a,4,8b-hexahydrocyclopentindole

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