1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

Base Information

Chemical Name:1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone
CAS No.:1265801-99-7
Molecular Formula:C₁₉H₁₈N₂O₃
Molecular Weight:322.364
Hs Code.:

Synonyms:1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

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Technology Process of 1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

There total 4 articles about 1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 78-94-4,25038-87-3
methyl vinyl ketone

: 3-oxo-3-phenyl-2-(2-phenylhydrazono)propanal

: 1265801-99-7
1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; at 100 ℃; for 0.0166667h; Microwave irradiation;
DOI:10.3998/ark.5550190.0012.225

Reference yield:

: 614-20-0
3-oxo-3-phenylpropionic acid

: 1265801-99-7
1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: water / 2 h / 0 - 5 °C

2: montmorillonite K₁₀ / methanol; water / 2 h / Reflux

3: nitrobenzene / 2 h / Reflux

4: 1,4-diaza-bicyclo[2.2.2]octane / 0.02 h / 100 °C / Microwave irradiation

With 1,4-diaza-bicyclo[2.2.2]octane; nitrobenzene; In methanol; water; 4: Baylis-Hillman reaction;
DOI:10.3998/ark.5550190.0012.225

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 1265801-99-7
1-(6-benzoyl-5-hydroxy-2-phenyl-2,3,4,5-tetrahydropyridazin-4-yl)ethanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; potassium hydroxide / 24 h / 20 °C

1.2: 0 - 5 °C

2.1: water / 2 h / 0 - 5 °C

3.1: montmorillonite K₁₀ / methanol; water / 2 h / Reflux

4.1: nitrobenzene / 2 h / Reflux

5.1: 1,4-diaza-bicyclo[2.2.2]octane / 0.02 h / 100 °C / Microwave irradiation

With 1,4-diaza-bicyclo[2.2.2]octane; water; nitrobenzene; potassium hydroxide; In methanol; water; 5.1: Baylis-Hillman reaction;
DOI:10.3998/ark.5550190.0012.225